Reaction calorimetry and high-pressure facilities

  • E459 Simular from HEL for evaluation of thermodynamics and reaction kinetics:
    • 1 litre double-jacketed glass vessel.
    • Combination pH electrode, automatic pH control, PT100 temperature probe, 150W internal heater, Julabo FP50HD refrigerated and heating circulator to control oil temperature
    • Controlled addition of solids liquids and gases
    • Turbidity monitoring
  • HEL AutoMate 130 bar pressure reactor with GC-MS sampling

Fractional distillation  (reactive distillation) facility

    • High performance pilot distillation unit, 5cm diameter column  packed with SULZER DX Hastelloy packing  giving 20 theoretical stage performance.
    • Can operate down to 2mBar.
    • To facilitate batch and fed batch reactive distillation studies the jacketed 1 litre reboiler vessel is also fitted with controlled dosing, agitation and is heated by recalculating oil
 

 

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